Microwave digestion method for phosphorus determination of fish tissue
نویسندگان
چکیده
منابع مشابه
Multi-syringe flow injection system with in-line microwave digestion for the determination of phosphorus.
A multi-syringe system for spectrophotometric determination of total phosphorus involving in-line digestion is proposed. Sample and digestion solution were dispensed and directed towards a digestion vessel located inside a domestic microwave oven (MWO) where sample digestion took place. Afterwards, the digested sample was merged with the necessary reagents for the colorimetric determination bas...
متن کاملRapid sample preparation for determination of iron in tissue by closed-vessel digestion and microwave energy.
We developed a rapid acid-digestion method for preparing tissue samples for iron determination. Specimens were digested in nitric acid and hydrogen peroxide under high temperature and pressure in closed Teflon vessels, with microwave energy. Analysis for iron in 25- to 250-mg portions of digested bovine liver powder (National Bureau of Standards Certified Reference Material no. 1577a) showed ex...
متن کاملPressurized Microwave Digestion Metal Determination of Biological Samples for
The utility of microwave oven for simple and rapid acid digestion of zoological and botanical materials was investigated by using a double Teflon vessel with a polypropylene jacket. The microwave-assisted digestion of samples with the HNO3-HCI-HCIO4-HF mixture in the bomb offers the advantage of taking much shorter process for sample preparation. The digestion was completed within 15 min even u...
متن کاملMicro-quantity tissue digestion for metal measurements by use of a microwave acid-digestion bomb.
We describe a simple and convenient method for processing small amounts of tissue samples for trace-metal measurements by atomic absorption spectrometry, by use of a modified Parr microwave digestion bomb. Digestion proceeds rapidly (less than or equal to 90 s) in a sealed Teflon-lined vessel that eliminates contamination or loss from volatilization. Small quantities of tissue (5-100 mg dry wei...
متن کاملRapid determination of chemical oxygen demand (COD) using focused microwave digestion followed by a titrimetric method.
water-pollution control analysis. It is closely related to the organic contamination level of a water or wastewater sample. The Cr-COD method is used as the standard in USA and Taiwan. Compared to Japanese Mn-COD method, it has a higher detection limit and severe chloride ion interference because of the stronger oxidant and the longer digestion time. In order to reduce the chloride-ion interfer...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Limnology and Oceanography
سال: 1999
ISSN: 0024-3590
DOI: 10.4319/lo.1999.44.3.0708